Assessment of dissolution techniques for the analysis of ceramic samples by plasma spectrometry

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dc.contributor	Universitat de Barcelona
dc.contributor.author	Tsolakidou, A.
dc.contributor.author	Buxeda i Garrigós, Jaume
dc.contributor.author	Kilikoglou, V.
dc.date	2013-01-21T20:17:30Z
dc.date	2013-01-21T20:17:30Z
dc.date	2002
dc.date	2013-01-21T20:17:30Z
dc.identifier.citation	0003-2670
dc.identifier.citation	196761
dc.identifier.uri	http://hdl.handle.net/2445/33464
dc.format	12 p.
dc.format	application/pdf
dc.language.iso	eng
dc.publisher	Elsevier B.V.
dc.relation	Versió postprint del document publicat a: http://dx.doi.org/10.1016/S0003-2670(02)01029-2
dc.relation	Analytica Chimica Acta, 2002, vol. 474, p. 177-188
dc.relation	http://dx.doi.org/10.1016/S0003-2670(02)01029-2
dc.rights	(c) Elsevier B.V., 2002
dc.rights	info:eu-repo/semantics/openAccess
dc.subject	Ceràmica antiga
dc.subject	Arqueometria
dc.subject	Química arqueològica
dc.subject	Pottery ancient
dc.subject	Archaeometry
dc.subject	Archaeological chemistry
dc.title	Assessment of dissolution techniques for the analysis of ceramic samples by plasma spectrometry
dc.type	info:eu-repo/semantics/article
dc.type	info:eu-repo/semantics/acceptedVersion
dc.description.abstract	In this study, 13 ceramic samples were subjected to dissolution using three different procedures: (a) acid attack in open PTFE vessels with a mixture of HF-HClO4, (b) fusion of the sample with lithium metaborate and (c) microwave digestion in PTFE bombs. The samples used in the study had been previously analyzed by neutron activation analysis (NAA), X-ray fluorescence (XRF) and X-ray diffraction (XRD) and they cover a wide range of ceramics fired in different atmospheres and temperatures as well as different mineralogical and chemical compositions. The effectiveness of each procedure is evaluated in terms of its ability to dissolve the various mineralogical phases of the samples, of the number of elements that can be determined and of the time needed for the whole scheme of analysis to be completed.

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