Microwave assisted synthesis of polynuclear Ni(II) complexes

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Title:	Microwave assisted synthesis of polynuclear Ni(II) complexes
Author:	Rosado Piquer, Lidia; Sañudo Zotes, Eva Carolina
Other authors:	Universitat de Barcelona
Abstract:	In this paper we test a solvent-free microwave assisted synthesis method with a known Ni7 complex, [Ni7(chp)12(OH)2(CH3OH)6] (2), and then extended the method to a more complex ligand system. We prepare two new trinuclear Ni(II) complexes ([Ni3(chp)4(tBuSALOH)2(MeOH)5] (4) and [Ni3(chp)4(iPrSALOH)2(MeOH)6] (5)) and report here their characterization and magnetic properties.
Subject(s):	-Complexos metàl·lics -Propietats magnètiques -Metal complexes -Magnetic properties
Rights:	cc-by-nc-nd (c) Elsevier Ltd, 2019 info:eu-repo/semantics/embargoedAccess http://creativecommons.org/licenses/by-nc-nd/3.0/es
Document type:	Article Article - Accepted version
Published by:	Elsevier Ltd
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