Synthesis of (E)-4-bromo-3-methoxybut-3-en-2-one, the key fragment in the polyhydroxylated chain common to oscillariolide and phormidolides A-C

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RECERCAT Home > Universitat de Barcelona > Química Inorgànica i Orgànica > Articles publicats en revistes (Química Inorgànica i Orgànica) > View document

To access the full text documents, please follow this link: http://hdl.handle.net/2445/98695

dc.contributor	Universitat de Barcelona
dc.contributor.author	Gil, Alejandro
dc.contributor.author	Lamariano Merketegi, Janire
dc.contributor.author	Lorente Crivillé, Adriana
dc.contributor.author	Albericio Palomera, Fernando
dc.contributor.author	Álvarez Domingo, Mercedes
dc.date	2016-05-19T15:16:32Z
dc.date	2017-05-17T22:01:27Z
dc.date	2016-05-17
dc.date	2016-05-19T15:16:37Z
dc.identifier.citation	0947-6539
dc.identifier.citation	658455
dc.identifier.uri	http://hdl.handle.net/2445/98695
dc.format	3 p.
dc.format	application/pdf
dc.language.iso	eng
dc.publisher	Wiley-VCH
dc.relation	Versió postprint del document publicat a: http://dx.doi.org/10.1002/chem.201600770
dc.relation	Chemistry-A European Journal, 2016, vol. 22, num. 21, p. 7033-7035
dc.relation	http://dx.doi.org/10.1002/chem.201600770
dc.rights	(c) Wiley-VCH, 2016
dc.rights	info:eu-repo/semantics/openAccess
dc.subject	Productes naturals
dc.subject	Síntesi asimètrica
dc.subject	Química orgànica
dc.subject	Natural products
dc.subject	Asymmetric synthesis
dc.subject	Organic chemistry
dc.title	Synthesis of (E)-4-bromo-3-methoxybut-3-en-2-one, the key fragment in the polyhydroxylated chain common to oscillariolide and phormidolides A-C
dc.type	info:eu-repo/semantics/article
dc.type	info:eu-repo/semantics/acceptedVersion
dc.description.abstract	The terminal bromomethoxydiene (BMD) moiety of the polyhydroxylated chain present in phormidolides and oscillariolides has been synthesized for first time. Several strategies for the stereoselective synthesis of the 4-bromo-3-methoxybut-3-en-2-ones are described. Furthermore, a preliminary study to successfully introduce this fragment within the polyol chain and introduction of the fatty acid allowed corroborate the end structure of the polyol.

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