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Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters Hayati, Payam Suárez García, Salvio Gutiérrez Alonso, Ángel Ruiz-Molina, Daniel Morsali, Ali Rezvani, Ali Reza Coordination polymer Sonochemical process Ultrasound irradiation Morphology One new lead(II) coordination supramolecular complex (CSC) (1D), [Pb(L)(I)], L = CHN (1-methyl imidazole), has been synthesized under different experimental conditions. Micrometric crystals (bulk) or nano-sized materials have been obtained depending on using the branch tube method or sonochemical irradiation. All materials have been characterized by scanning electron microscopy (SEM), powder X-ray diffraction (PXRD) and FT-IR spectroscopy. Single crystal X-ray analyses on complex 1 showed that Pb ion is 4-coordinated. Topological analysis shows that the complex 1 is 2,3,5C2 net. Finally, the role of reaction time and temperature on the growth and final morphology of the structures obtained by sonochemical irradiation have been studied. 2018 Article https://ddd.uab.cat/record/220658 urn:10.1016/j.ultsonch.2017.11.033 urn:oai:ddd.uab.cat:220658 urn:scopus_id:85036479536 urn:articleid:18732828v42p320 urn:wos_id:000426021200035 urn:icn2uab:3126123 eng Ministerio de Economía y Competitividad MAT2015-70615-R Ministerio de Economía y Competitividad SEV-2013-0295 Ultrasonics sonochemistry ; Vol. 42 (April 2018), p. 320-326 open access Aquest document està subjecte a una llicència d'ús Creative Commons. Es permet la reproducció total o parcial, la distribució, i la comunicació pública de l'obra, sempre que no sigui amb finalitats comercials, i sempre que es reconegui l'autoria de l'obra original. No es permet la creació d'obres derivades. https://creativecommons.org/licenses/by-nc-nd/4.0/ application/pdf