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Preparation of alpha-labeled aldehydes by base-catalyzed exchange reactions
Ariza Piquer, Xavier; Asins Muñoz, Guillermina; García Gómez, Jordi; García Hegardt, Fausto; Makowski, Kamil; Serra i Cucurull, Dolors; Velasco Turbau, Javier
Universitat de Barcelona
A simple, efficient protocol for the preparation of α-labeled aldehydes based on H/D exchange catalyzed by 4-(N,N-dimethylamino)pyridine or Et3N is described. High chemical yields and ratios of isotope incorporation were obtained even when small amounts (1 mmol) of aldehyde were used.
Trastorns del metabolisme dels lípids
Bioquímica
Aldehids
Disseny de medicaments
Medicina nuclear
Lipid metabolism disorders
Biochemistry
Aldehydes
Drug design
Nuclear medicine
(c) John Wiley & Sons, 2010
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